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Beilstein J. Org. Chem. 2006, 2, No. 21, doi:10.1186/1860-5397-2-21
Graphical Abstract
Figure 1: Thiazolidine-2,4-dione mimic & chosen lead scaffold.
Scheme 1: Reagents and conditions: (a) PS-PPh3, DEAD, THF, rt, 16 h, 54%.
Figure 2: Proposed mechanism of the Mitsunobu reaction.
Scheme 2: Reagents and conditions: (a) PS-PPh3, ADDP, THF, rt, 16 h, 81%.
Scheme 3: Reagents and conditions: (a) 1 N aq. NaOH, MeCN, 100°C μW, 10 mins, 96%.